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Articles

Analysis of Microplastics using FTIR and Raman-Microscopy (2)

The omnipresent occurrence of microplastics and the expected consequences are subject of modern research and the topic receives more and more public awareness. Due to the fact that plastic waste is degrading only very slowly the amount of microplastics in the environment is steadily increasing.

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In particular, the contamination of the world‘s oceans is a problem. Currently, an annual entry of microplastics into the world‘s oceans of about 210 g per person or a total of approximately 1.5 megatons is estimated.[1] The uptake by marine organisms and fish results in a contamination of the human food-chain through microplastics including substances such as plasticizers or adsorbed pollutants.

According to definition, polymer particles with a diameter of less than 5 mm are referred to as microplastics particles (MPP). Depending on their origin, they are further subdivided into primary and secondary particles. Primary particles are those which are specifically produced industrially like for instance peeling particles in cosmetic products. Secondary microparticles are formed by physical, biological and chemical degradation of macroscopic plastic parts and are the main source of all released microparticles. They are mainly formed by the degradation of improperly disposed plastic waste, tire abrasion and washing of synthetic textiles.

Keywords

Instrumentation and Software

Microplastics

HYPERION FTIR Microscope

Particle analysis

SENTERRA II Raman Microscope

Polymers

OPUS Spectroscopy Software

A high sample throughput combined with reliable identification of even the smallest particles is possible with Microspectroscopic FTIR . This methods are universally applicable and permit the selective analysis of individual particles with a size of a few micrometers. The rapid analysis of larger accumulations of microplastics particles is also possible by means of automated grid measurements.

FTIR analysis of microplastics

Fourier transform infrared (FTIR) spectroscopy is a proven method for the identification of all types of polymers. It allows a reliable differentiation between substances of natural and synthetic origin and allows determining the polymer type (see figure 1). Typically, the identification is carried out by means of an automated comparison against extensive spectral libraries.

With conventional FTIR spectrometers, it is already possible to easily examine larger microparticles. In comparison, FTIR microscopy allows the analysis of single particles with a size of only a few micrometers. Depending on the size of the particle, it is even possible to record several spectra at different points on a single particle.

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Categories
Articles

Analysis of Microplastics using FTIR and Raman-Microscopy

The omnipresent occurrence of microplastics and the expected consequences are subject of modern research and the topic receives more and more public awareness. Due to the fact that plastic waste is degrading only very slowly the amount of microplastics in the environment is steadily increasing.

kura2

In particular, the contamination of the world‘s oceans is a problem. Currently, an annual entry of microplastics into the world‘s oceans of about 210 g per person or a total of approximately 1.5 megatons is estimated.[1] The uptake by marine organisms and fish results in a contamination of the human food-chain through microplastics including substances such as plasticizers or adsorbed pollutants.

According to definition, polymer particles with a diameter of less than 5 mm are referred to as microplastics particles (MPP). Depending on their origin, they are further subdivided into primary and secondary particles. Primary particles are those which are specifically produced industrially like for instance peeling particles in cosmetic products. Secondary microparticles are formed by physical, biological and chemical degradation of macroscopic plastic parts and are the main source of all released microparticles. They are mainly formed by the degradation of improperly disposed plastic waste, tire abrasion and washing of synthetic textiles.

Keywords

Instrumentation and Software

Microplastics

HYPERION FTIR Microscope

Particle analysis

SENTERRA II Raman Microscope

Polymers

OPUS Spectroscopy Software

A high sample throughput combined with reliable identification of even the smallest particles is possible with Microspectroscopic FTIR . This methods are universally applicable and permit the selective analysis of individual particles with a size of a few micrometers. The rapid analysis of larger accumulations of microplastics particles is also possible by means of automated grid measurements.

FTIR analysis of microplastics

Fourier transform infrared (FTIR) spectroscopy is a proven method for the identification of all types of polymers. It allows a reliable differentiation between substances of natural and synthetic origin and allows determining the polymer type (see figure 1). Typically, the identification is carried out by means of an automated comparison against extensive spectral libraries.

With conventional FTIR spectrometers, it is already possible to easily examine larger microparticles. In comparison, FTIR microscopy allows the analysis of single particles with a size of only a few micrometers. Depending on the size of the particle, it is even possible to record several spectra at different points on a single particle.

figure3
figure1
Categories
Articles

MPA II Multi Purpose FT-NIR Analyzer

The FT-NIR spectrometer MPA II is designed to meet the demands of today’s and tomorrow’s quality control. It combines outstanding flexibility and high performance with an easy-to operate interface.

The FT-NIR spectrometer MPA II is designed to meet the demands of today’s and tomorrow’s quality control. It combines outstanding flexibility and high performance with an easy-to operate interface.

  • Full line of sample presentation options for all NIR applications
  • Software-controlled module selection, no manual exchange required
  • Low cost of ownership thanks to high quality components with long life time
  • Easy calibration transfer to other Bruker lab, at-line or process spectrometers
  • Fully cGMP and 21 CFR Part 11 compliant, supports validation according to USP <1119> and Ph.Eur 2.2.40

Maximum Flexibility

The MPA II offers everything you need for the analysis of liquids, semi-solids, solids, powders and tablets:

  • Sample compartment
  • Integrating sphere
  • Fiber optic probes
  • Transmission unit

With powerful accessories like the automated 30-position sample wheel for vials and tablets, the sample rotator for the integrating sphere and many different fiber probes, you will achieve high sample throughput with excellent precision.

High Performance FT-NIR

The MPA II incorporates state-of-the-art optics for outstanding sensitivity and stability. The heart of the instrument is Bruker‘s permanently aligned RockSolidTM interferometer with gold-coated optics for maximum efficiency and sensitivity. The permanent alignment provides consistent high quality results, less downtime and outstanding stability; a precondition for reliable results and successful calibration transfer.

Built to Last

Made from robust components, using state-of-the-art solid state laser technology: the MPA II is a future-proof investment. This is why it comes with 10-year warranty on the moving parts of the interferometer as well as on the laser.

Hassle-Free Maintenance

The MPA II spectrometer is designed to be easily maintained by the user, decreasing downtime and maintenance costs. Light source and desiccant cartridge are easily interchangeable and permanent online diagnostics monitor the instrument and advise the user of any problems.

Service and Support

If you need us, we are here to help! Bruker Optics is staffed with a large group of scientists and engineers to respond to your needs:

  • Applications support
  • Comprehensive training courses
  • Worldwide service

Easy Operation

Customizable workspaces as well as easy measurement modes which guide you through the setup of analytical methods are standard in the OPUS spectroscopy software. Measurements can be started with a mouse click or at the touch of a button.

Software

The OPUS measurement software with integrated database support and additional OPUS packages make the MPA II easy to operate:

  • OPUS/NIRLAB: Dedicated QA/QC software combining OPUS/LAB with qualitative and quantitative evaluation routines
  • ONET: Web based application to setup, administrate and control a network of FT-NIR instruments from anywhere in the world
  • OPUS/IDENT: Setup of identification methods with hierarchical libraries
  • OPUS/CONFO: Setup of conformity test methods
  • OPUS/QUANT: Setup of self-optimizing chemometric quantification methods

Application

The application of MPA II:

  • Agriculture
    • Grain & Oil Seeds Analyzer
    • Biofuel Analyzer
    • Tobacco Analyzer
    • Sugar Analyzer (Brix, Pol)
    • Soil Analyzer
  • Food
    • Milk & Dairy Analyzer (Raw Milk, UHT, Cheese, Sour Cream, Ice Cream, Yoghurt, Milk Powders, Butter, Cream, Condensed Milk, Whey, Whey Cream, Whey Butter, Whey Protein Concentrate, and Lactose)
    • Meat & Sausages Analyzer
    • Oils & Fats Analyzer
      • Edible oils (Iodine Value (IV), Anisidine Value (AV), Free Fatty Acid (FFA), Trans Fatty Acid (TFA))
      • Palm Oil, Palm Kernel Oil, (Crued Palm Oil (CPO), Palm Olein, Palm Sterin, etc
    • Beverages Analyzer
    • Confectionary Analyzer
    • Flour & Milling Analyzer (moisture, protein, ash)
    • Cereals Analyzer
    • Condiments Analyzer
  • Feed
    • Feed & Forage Analyzer
    • Feed ingredients Analyzer
    • Pet Food Analyzer
    • Fish feed Analyzer

Validation

Trust your results with Bruker Optics’ OPUS/VALIDATION package and the OPUS spectroscopy software:

  • Full 21 CFR Part 11 compliance
  • Full GMP compliance
  • IQ/OQ/PQ support

Bruker is a NASDAQ listed company and has most of their manufacturing facility around the globe, mainly in Germany. Bruker is a manufacturer of scientific instruments for materials research, as well as for industrial and applied testing field. Their range of product is ranging from X-rays like XRD, XRF, SAXS, Single Crystal XRD, X-ray micro CT. Another range would be the IR Spectrometer and NIR spectrometer who serve broad range of field from Polymer and Plastic, Pharmaceutical, Automotive and Electronics, Food and Feed, Milk and Dairy, Chemical and Petrochemical, Edible Oil and many others. PT. Dynatech International is the distributor of Bruker in Indonesia.

Categories
Articles

The Foundry Master Pro II Optical Emission Spectrometer

Superior metals analysis without compromise

Seamless quality control is essential throughout the metals industry, from trace element analysis in scrap metal, to incoming materials inspection, melt process control and goods issue.

The FOUNDRY-MASTER Pro2 optical emission spectrometer is a metals analyser engineered to deliver superior analysis at every stage, without compromising your productivity. Thanks to its near constant availability and high resolution dynamic detector you can get detailed results quicker, minimising production downtime and costly errors.

A cost effective choice, the FOUNDRY-MASTER Pro2 minimises argon consumption and keeps down operating costs.

This unique combination of performance and efficiency makes FOUNDRY-MASTER Pro2 the analysis instrument of choice for the metals industry.

Highlights and applications

The intuitive user interface and numerous features of the FOUNDRY-MASTER Pro2 make analysis work easy. Just place the sample on the spark stand, start the measurement and read the result. The extremely low detection limits for various applications, particularly carbon and nitrogen analysis in iron and steel, offer superior results in QA/QC and melt process control.

  • Maximum availability, minimum downtime.
  • Excellent long-term stability, precision and accuracy.
  • Increased productivity with higher sample throughput.
  • Low cost of ownership with optimised power and argon consumption.
  • Includes largest metals database on the market for fast and easy grade identification.
  • Method for determination of soluble and insoluble aluminium available.

A unique spark stand, accessible from three sides, makes the FOUNDRY-MASTER Pro2 ideal for samples with complex and irregular shapes and sizes.

Our Service

Our global network of service hubs offers a full range of technical support to keep you up and running.

  • Telephone help-desks

For a fast response to your problem.

  • Consumables and accessories

From electrodes to spare part kits.

  • Recertification and maintenance

Ensures your analyser produces the right result year after year.

  • Training

Understand your analyser and its features.

  • Extended warranties

Avoid unplanned costs.

  • Repairs

Fast and efficient turnaround.

The largest metals database on the market for fast and easy grade identification is already installed on the FOUNDRY-MASTER Pro2.

The Hitachi GRADE Database offers more than 12 million records for over 339,000 materials from 69 countries and standards. You can update your instrument’s grade database with a few clicks – no time consuming research in norms and grade catalogues.

This product is formerly an Oxford Instruments Brand. Oxford Instruments plc, a leading provider of high technology solutions, information and services for industry and research, announced on 26 April 2017 that it has agreed to sell its Industrial Analysis business to Hitachi High-Technologies Corporation (‘HHT’) for a consideration of £80 million on a cash and debt free basis. HHT will acquire the companies, assets and liabilities that comprise the Industrial Analysis business.

The Industrial Analysis business is a leading global provider of handheld and bench-top instruments using X-ray Fluorescence (XRF), Laser Induced Breakdown Spectroscopy (LIBS) and Optical Emission Spectroscopy (OES) technologies for analysing materials in a broad range of industrial applications. Headquartered in Oxford, UK, the Industrial Analysis business has research and development and assembly operations in Finland and Germany and sales and support operations in a number of countries around the world. PT. Dynatech International was formerly the distributor of Oxford Instruments in Indonesia and now is the distributor of Hitachi High-Technologies Corporation in Indonesia.

Categories
Articles

Hexagon Manufacturing Intelligence Releases PC-DMIS 2018 R1

HexagonMFG 2
Hexagon Manufacturing Intelligence today launched PC-DMIS 2018 R1, the latest edition of the world’s most popular measurement software. This is the first of two major releases scheduled for PC-DMIS in 2018, with continued service pack updates to ensure maximum reliability of the platform.

 

PC-DMIS 2018 R1 allows users to easily convert AutoFeatures to points or quickly use the measured hits for new Constructions and Dimensions, available for Plane, Circle, and Cylinder AutoFeatures. By converting each hit to a vector point, Optimize Path can be used to enhance the order of point measurement, reducing the number of probe tip changes and overall measurement time. New support for Q-DAS Traces enables easier analysis of PC-DMIS data. The new QuickSet control allows users to use both QuickFeature and GD&T Selection and still have the ability to modify measurement strategies. 

“With PC-DMIS 2018 R1, we fulfil our commitment to add the most highly-requested items from the user ‘Idea Center’,” states Ken Woodbine, Product Line Manager for Metrology Software at Hexagon Manufacturing Intelligence. “These include the graphical point manipulation feature, and the ‘push to points’ AutoFeature functionality. We also introduce seamless integration with the industry-standard Q-DAS software so key process parameters affecting quality can be easily identified and tracked. Additionally, we focus on optimising key elements of the measurement routine creation workflow, including front and centre visual access to key measurement strategy parameters with our new QuickSet widget technology.”

Enhanced speed of QuickFeature measurement enables users to create multiple circles and cylinders with just one click, optimised for bolt hole patterns or whenever surfaces contain multiple features of the same size and shape. The latest edition also introduces improved Flush and Gap AutoFeature workflow for point cloud inspection. This improved workflow makes it even faster to extract multiple Flush and Gap AutoFeatures from an existing cloud of points object, most helpful when inspecting sheet metal seams. INSPECT has also been improved to include CAD and LIVE views from PC-DMIS and the ability to create Playlists including one or more routines to be executed a specified number of times.

Other notable improvements within PC-DMIS include a new CAD Rotation Widget for resizable one-click CAD rotation, Added (M) for Coaxiality/Concentricity, Leica Absolute Scanner LAS laser scanner support, improved 4K monitor support, improved QuickFeature laser support, Datakit 2017.3 implementation, user interface refresh, and improved tracker user experience.

PC-DMIS 2018 R1 is available to download immediately. More information is available through local Hexagon commercial operations and dealers.

 
About Hexagon Manufacturing Intelligence

 

Hexagon Manufacturing Intelligence helps industrial manufacturers develop the disruptive technologies of today and the life-changing products of tomorrow. As a leading metrology and manufacturing solution specialist, our expertise in sensing, thinking and acting – the collection, analysis and active use of measurement data – gives our customers the confidence to increase production speed and accelerate productivity while enhancing product quality.

Through a network of local service centres, production facilities and commercial operations across five continents, we are shaping smart change in manufacturing to build a world where quality drives productivity. For more information, visit HexagonMI.com.

Hexagon Manufacturing Intelligence is part of Hexagon, a leading global provider of information technologies that drive productivity and quality across geospatial and industrial enterprise applications.

Hexagon’s solutions integrate sensors, software, domain knowledge and customer workflows into intelligent information ecosystems that deliver actionable information. They are used in a broad range of vital industries.

Hexagon (Nasdaq Stockholm: HEXA B) has approximately 18,000 employees in 50 countries and net sales of approximately 3.1bn EUR. Learn more at hexagon.com and follow us @HexagonAB.

Categories
Events

Manufacturing Indonesia 2017

Manufacturing Indonesia is Asia’s largest international manufacturing exhibition providing a professional business platform for Indonesia’s manufacturing industry.

Manufacturing Indonesia is well known and respected among industry professionals. The show attracts industry leaders and key players in the global manufacturing industry who want to showcase their latest products and services in one venue, the Jakarta International Expo

Manufacturing Indonesia 2017 was again held in Jakarta International Expo Kemayoran, 06 – 09 December 2017. PT. Dynatech International have been participated in this prestigious exhibition for years and this year PT. Dynatech International booth is located in  Hall D-8814.

In this event PT. Dynatech International not only displaying the latest innovation from manufacturer that represented by our company but also showcasing the a few latest addition of manufacturer such as Bruker, Solartron (member of AMETEK group) & Phenom (newly acquired by Thermo Fisher Scientific). PT. Dynatech International is honored to represent those reputable companies as their distributor for Indonesia region. 

In Short Bruker is a NASDAQ listed company and has most of their manufacturing facility around the globe, mainly in Germany. Bruker is a manufacturer of scientific instruments for materials research, as well as for industrial and applied testing field. Their range of product is ranging from X-rays like XRD, XRF, SAXS, Single Crystal XRD, X-ray micro CT. Another range would be the IR Spectrometer and NIR spectrometer who serve broad range of field from Polymer and Plastic, Pharmaceutical, Automotive and Electronics, Food and Feed, Milk and Dairy, Chemical and Petrochemical, Edible Oil and many others.

Phenom-World, which is based in Eindhoven, the Netherlands, delivers world leading desktop SEM (Scanning Electron Microscope) and imaging and analysis packages, for both research and industrial worlds. At the end of 2017, Thermo Fisher Scientific Inc., the world leader in serving science, announced it has completed the acquisition of Phenom-World. Thermo Fisher will integrate the business into Thermo Fisher’s Analytical Instruments segment. This great addition of Phenom World’s leading desktop SEM platform strengthens Thermo Fisher’s leadership in electron microscopy and expands the company’s entry-level and desktop SEMs offerings for customers working in the materials science, industrial manufacturing, life sciences, electronics industries and education & research sector.

There are hundreds of visitors dropped by to PT. Dynatech International’s booth during the 4 days event and besides they get in depth inside of the cutting edge technology from different manufacturer represented by PT. Dynatech International, they also experience the warm courtesy of Dynatech’s Support team.

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Categories
Articles

Rockwell Hardness Tester FR-X Series

Since our establishment in 1995, FUTURE-TECH CORP. has been producing a variety of hardness testers and accessories and supplying them to not only the domestic market of Japan but also more than 35 countries around the world. Our special trademark is showing our customers value.

Continuing the Success of its predecessor of FR Series, FUTURE-TECH CORP is proud to introduce the new series of Rockwell Hardness Tester FR-X Series. The new series is obtained by supreme precision and reliability. It also adopts entirely new design as well as precision manufacturing, which based on newly set up advanced manufacturing. By the adoption of stealth type double information panel, improved the remarkable visibility and operation.

To Learn more about the new system or to get a demonstration by our application specialist please contact us.

Categories
Articles

ALPHA II – The New Benchmark for Compact FTIR Spectrometers

The ALPHA II is the enhanced follow-up model of its very successful predecessor. It combines outstanding quality with compactness and user convenience. With its integrated touch panel PC and the intuitive OPUS-TOUCH software, the IR analysis gets easier than ever. 

Owing to several technical innovations, the ALPHA II provides higher sensitivity, higher spectral resolution, extended spectral range and further increased robustness. 

The broad range of QuickSnapTM sampling modules allows the analysis of almost any kind of sample, each with a perfectly matched instrument configuration. The ALPHA II offers all the capabilities needed for efficient routine analysis. It is ideally suited for quality control tasks in industrial manufacturing. 

Learn more about the ALPHA II: 
 

Categories
Articles

Nickel Ore

BRUKER S2 PUMA

for fast and reliable Analysis of Nickel Ore (Nickel Laterite) by EDXRF. For a long time the main source for the nickel metal production was magmatic sulfide ore. But with the globally increased demand of nickel metal other sources become more needful.

Mining Site

For a long time the main source for the nickel metal production was magmatic sulfide ore. But with the globally increased demand of nickel metal other sources become more needful. One of these nickel sources is laterite which is typically mined as low- grade deposit in open pit mines. Due to their large dimensions these mines usually contain a significant amount of nickel and therefore they contribute more and more to the increasing nickel demand. In order to optimize the nickel production processes the monitoring of the chemical composition of nickel laterite and its associated materials is more than ever essential. Besides the major elements such as Ni, Fe, and Si the elements Mg, Al, Ca, Ti, Cr, Mn, Co, Cu, and Zn typically occur in minor and trace amounts.

All these elements can be analyzed using the
 S2 PUMA energy-dispersive X-ray fluorescence (EDXRF) spectrometer. This instrument offers a fast and accurate control of both the mining process and the subsequent beneficiation processes.

For these Bruker Center of Excellence in Singapore has performed an Analysis involving measurements with an S2 PUMA with standard XFlash detector and a Pd target X-ray tube was used.  For fast process control the samples were prepared as pressed pellets. Due to the simple and straightforward sample preparation the analytical results are available within minutes after taking the sample. A set of 15 international certified reference materials (CRMs) were used to prepare the calibration for the 12 elements. For fast process control the samples were prepared as pressed pellets. Due to the simple and straightforward sample preparation the analytical results are available within minutes after taking the sample.

The data acquired by the measurement above has proved the high performance of the EDXRF spectrometer to test or analyze of Nickel Ore/Nickel Laterite. The EDXRF used for this measurement is manufactured by Bruker and the model used for this experiments is S2 PUMA with HighSense technology and XFlash detector . With a set of 15 standards the 12 most important elements in nickel ore samples can be determined. If you interested to learn more about the application above, please contact us.

Categories
Articles

AICON Photo Scanner

The company CMA, service provider for automotive development, has made a video showing pre- and post-crash measurement with AICON MoveInspect XR8.

2AICON

The company CMA, service provider for automotive development, has made a video showing pre- and post-crash measurement with AICON MoveInspect XR8. Quick setup, easy calibration, effortless measuremernt and highly precise results – the AICON MoveInspect XR8 is the right solution for assembly, fixture setup, wireless probing, and dynamic deformation analysis.

Our Advantage :

  • Very fast Reverse Engineering
  • Friendly user Software
  • Precision 3D Scan
  • Solution for Car Automotive Maker, Aeroscpace, Medical, Mold Maker etc
  • Easy to use